Specifications include, but are not limited to: Item 1: Soils/Non-Aqueous Item 2: Aqueous A. EPA SW-846 Method 802 IB – Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors; B. EPA SW-846 Method 8260C – Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) GC/MS constituents as listed in the method plus MTBE; C. EPA SW-846 Method 82700 – Semi volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) as listed in the method plus 1- methylnaphthalene and 2-methylnaphthalene; D. EPA SW-846 Method 8310 – Polynuclear Aromatic Hydrocarbons (Note: method 8270 SIMS allowed if detection limits meet or exceed WQCC numerical standards.); E. EPA SW-846 Method 6010C/6020A – Metals Inductively Coupled Plasma-Atomic Emission Spectrometry (dissolved); F EPA SW-846 Method 7470A/7471B – Mercury (dissolved); G. General Chemistry (Cations and Anions) methods from 40 CFR 136.3 to include: fluoride (EPA Method 300); calcium (Method 6010C); potassium (EPA SW-846 Method 6010C); magnesium (EPA SW-846 Method 6010C), sodium bicarbonate (EPA Method 310.1), carbonate (EPA Method 310.1), chloride (EPA Method 300.0, 300.1, or SM 4500B), sulfate (EPA Method 300.1), total dissolved solids (EPA Method 160.1) for aqueous only, cation/anion balance (EPA Method 300), pH (EPA Method 150. I), specific conductivity (EPA Method 120.I), and bromide (EPA Method 320.1); H. EPA SW-846 Method 8015-M (GRO/DRO/MRO), Nonhalogenated Organics by Gas Chromatography Petroleum Hydrocarbons; I. EPA Method 418.1 – Total Extractable Petroleum Hydrocarbons (TPH) or other OCD/EMNRD approved method; J. EPA Method 405.1 – Biochemical Oxygen Demand (BOD); and K. EPA Method 410.1 – Chemical Oxygen Demand (COD). Awarded Vendor shall provide the following type and number of containers with the specified preservative. • Soils/Non-Aqueous: 3 x 4-ounce glass jars with Teflon lined screw cap, no preservative; • Aqueous: VOCs 3 x 40 mL VOAs with HCL; • SVOCs 1 x I L glass, no preservative; • Metals I x 500 mL plastic with HN03; • General Chemistry 1 x I L plastic, preservative ; • GRO 3 x 40 mL VOAs with HCL; • DRO 3 x 40 mL VOAs with HCL; • TPH 1 x I L glass with HCL; • BOD 1 x I L HDPE, no preservative; and • COD 1 x 250 mL HDPE with H2SO4.
